Method Wizard Step 2 - Temperature Assistant, Connectivity Software solutions Data flow from one instrument to another, Productivity (released time from the team) Uptime Optimize processes, Reduction in operating costs Total cost of ownership Maintenance cost reduction, Shift to the next level measurement process (from manual to automated, or to on-line measurement; automation), Sustainable design (futureproof modular design long lasting), Time reduction quick adjustment and scalability of methods, User skills and knowledge (theory of applications, technologies, methods, tips and tricks), Metal, Plastic and Electronics Components, Download the Reference Paper on Methods for Halogen Moisture Analyzers, WhitePaper Drying oven versus moisture analyzer, Method Development Support & Application Search, Download the Drying Oven vs. Halogen Moisture Analyzer Guide. Weigh the empty dish and lid. USP <731> ("Loss on Drying"), AOAC and ISO describe thethermogravimetric method using a drying oven as a standard procedure for determining moisture content. Good labelling is key. Which method is best for you, depends on how fast you need the result or if you need the result using an official method. METTLER TOLEDO is an expert in moisture analysis and offers a wide range of reliable and easy to use moisture analyzers to suit the needs of quality control, production and in-process control of many industries, such as pharma, plastics and the food industry. NIR has been applied to moisture content analysis of a wide variety of food commodities and is an official method for moisture content determination in dried vegetables (AOAC Method 967.19). Equipment upgrades from the existing AOAC standard methods provide safer more efficient methods of analysis. Weigh the empty dish and lid. Evaporate the solvent by using the vacuum condenser. /img0 73 0 R Calculation Protein (%) = (A-B) N 1.4007 6.25 W Where A = volume (ml) of 0.2 N HCl used sample titration B = volume (ml) of 0.2 N HCl used in blank titration N = Normality of HCl W = weight (g) of sample 14.007 = atomic weight of nitrogen 6.25 = the protein-nitrogen conversation factor for fish and its by-products 3. This is a common misconception. stream 4. 3. Continue to dry until the readout on the scale is constant (30-45 mins). endobj It can be represented as w. Ww = Weight of water content present in the sample, Ws = Weight of solid particles present in the sample. 27 0 obj <>/Filter/FlateDecode/ID[<7749ED4275BB7F4F8AE00EC394F8CE44>]/Index[10 38]/Info 9 0 R/Length 86/Prev 29391/Root 11 0 R/Size 48/Type/XRef/W[1 2 1]>>stream Manual processes are more prone to error so it's best to use the built-in balance application or a software solution (LabX) with a balance to capture all the results and do the calculations automatically. 6. Everything which evaporates upon heating is named moisture. The formula is often used in connection with tables in Methods 82-21.01, 82-22.01, and 82-23.01. SCOP. There are many stages of the production process where moisture determination benefits the overall quality of the finished product: raw materials, goods-in, storage, in process control, QC, packaging, etc. There is no one-size-fits-all method for moisture content determination as the samples vary greatly in properties. Weigh about 3 g of sample to the dish. The weight loss due to vaporization of water is taken as the weight of moisture. Six different methods were compared in this study. USP 731 <loss on drying>, AOAC and ISO describe the thermogravetric method using a drying oven as a standard procedure for determining moisture content. However, thereference method for loss on drying (drying oven method) can take many hours to reach a result. Continual determination of mass during drying process. >> Weigh about 3 g of sample to the dish. 6. This is the standard against which other methods are compared. Spread the sample with spatura. By validating the results of halogen moisture analysis against those from the drying oven, companies can benefit from a convenient and compliant alternative loss on drying solution. /T1_3 19 0 R If you already have a reference value (e.g. I have many different samples (liquid, paste-like, solid, powder). In most cases, the moisture analyzer can deliver an equivalent loss on drying moisture result, and typically better repeatability, in much less time, making it a fast alternative to USP <731> ("Loss on Drying") and ASTM D6980 Standard Test Method for Determination of Moisture in Plastics by Loss in Weight and other industry standards. Information about and monitoring of moisture content is therefore very important. The temperature at which the sample is oven-dried ranges from 110oC +- 5oC. Report loss in weight as moisture. Explore the links below to see our wide range of tools and our application method library. 2. This method determines moisture and any materials that are volatile under conditions of test. Alternatively, electrical devices, referred to as moisture meters or moisture testers, are employed. How do I develop a loss on drying method on my moisture analyzer for my substance? drying oven procedure). However, the reference method for loss on drying (drying oven method) can take many hours to reach a result. After drying, transfer the dish with partially covered lid to the desiccator to cool. . The most important is variability of the heating temperature, followed by the weighing performance. Calculate percentage moisture (wt/wt) as described below. No balance or desiccator required Suitable for at-Iine use, Substances other than water may evaporate. They describe the amount of material remaining after all the moisture has been evaporated. Weigh the empty dish and lid. *PSoG;RMj)3S*82111 Laboratory Determination of Moisture Content of Soils AASHTO Designation: T 265-15 1. For full access to this pdf, sign in to an existing account, or purchase an annual subscription. After a sufficient period, remove the sample from the oven and place it in the desiccator for cooling the sample. The LabX report generator enables you to create elegant reports with charts which can be printed out or saved electronically. %PDF-1.5 % 58 Special Properties of Fats, Oils, and Shortenings Methods, 48 Oxidizing, Bleaching, and Maturing Agents Methods, 66 Semolina, Pasta, and Noodle Quality Methods. When compared with the same samples dried to constant weight in an atmospheric oven at 100C the vacuum dried product will show a 10 to 50% greater loss of weight depending on carbohydrate content. The method is accurate but time consuming. Our reference paper will guide you through the setup of a robust moisture method for your sample including the right sample preparation and sample application. /Type /Page When fumes are no longer produced, place crucible and lid in furnace. << Weigh about 5 g sample into the crucible. To determine the moisture content of fats and oils by moisture distillation. /Rotate 0 . h{Qxgqh.$J:FYQ/,\=,DU9>c >1per{ 4OvekUN.^l}E9~r+HZtc ^B~v.|o)ZoYo>kQWv,b e?|t:b#-`]. Results can be printed out for your lab journal or saved on a USB stick to be saved electronically. After that, the sample is placed in a thermostatically drying oven that is maintained at a temperature of 110, A period of 16 to 24 hours is sufficient but it also varies with the. To find your application use the filters for 'Sample', 'Industry' or use full text search. 5. Place the dish with sample in the oven. The total fat. Heating of sample by convection. The methods are applicable to flour, semolina, bread, all kinds of grains and cereal products, and food products (except those that are sugar coated). If your batch number is a barcode, you can even connect a barcode reader to scan it, or any other ID. Moisture Control Design Analysis in Buildings There was an error retrieving our menu. . See how easy it is to measure the moisture content of pharmaceuticals in the lab or directly on the production floor with a halogen moisture analyzer. To determine the amount of low molecular weight volatile material in most fats and oils. If not, return the crucible and lid to the furnace for the further ashing. Learn how moisture analyzer is used to reliably measure the dry content in chemical industry. Cheese sample preparation using an Oster blender yielded consistently lower variance in final moisture content than did preparation of cheese samples with a hand grater, rotary grater, and plug and plunger. If you own a METTLER TOLEDO moisture analyzer (HX204, HS153 or HC103) use the integratedMethod Wizardfunctionality that guides you step-by-step to a reliable moisture method with minimum effort. Loss on Drying. How do the results on the moisture analyzer compare to the standard method? 4. for I am using the drying oven procedure. The moisture content is determined by weighing the sample before and after drying and determining the difference. Place the lid after complete heating to prevent loss of fluffy ash. /Parent 1 0 R Dry the empty dish and lid in the oven at 105 C for 3 h and transfer to desiccator to cool. Apparatus (see AOAC Official Method 934.06) 5.1 Analytical balance sensitive to 1 mg or better. endobj /Type /Page Cool down in the desiccator. 143 4. Manufacturers of these instruments will furnish conversion tables for their use, but instruments should be calibrated under conditions of actual use in comparison with oven methods. The accuracy of a moisture analysis result may be influenced by several factors. Take advantage of METTLER TOLEDO's moisture analysis expertise to improve your moisture analysis processes. Different industries use different units e.g. The moisture content is determined by measuring the mass of a food before and after the water is removed by evaporation. 4. Place the dish with sample in the oven. This method determines moisture content in flour and semolina. This method is not suitable for thermally unstable compounds. hb```5@(AcWe& ~?P#n Tsw`XKiPQD^-9Np1QT METTLER TOLEDO's application databasecontains over 150 free ready-to-use cross-validated drying methods. Is there a difference between dry content (DC) and total solids (TS). So, moisture content can be determined as: Moisture content = [(W2 W3) / (W3 W1)] * 100. Moisture content (AOAC, 1999) Method 1. Soils that contain gypsum or other minerals which have a loose bond with water, moisture content for these. AOAC Official Method 984.20 Loss on Drying (Moisture) and Volatile Matter in Oils and Fats: Karl Fisher Method. /Im0 21 0 R /Type /Page The European Pharmacopeia has recently updated Chapter 2.2.32, "Loss on Drying", to include halogen moisture analyzers as an acceptable alternative to the drying oven reference method. Weigh the empty dish and lid. Please reload the page. Determination of moisture content (AOAC, 1999) Method 1. When using a moisture analyzer, the sample heats up and dries by absorbing infrared radiation from the heating element. LabX saves everything in a secure database so you can be sure your data is safe. 7. The term "apparent moisture" is vised becavise oven drying also causes loss of volatile organic material. %%EOF 4 Apparatus Usual laboratory equipment and, in particular, the following. ); (2) to compare the effects of drying temperature, time, and sample treatment in an air oven on the moisture content of pearl millet using . The chemical reaction of water with a Karl Fischer reagent (containing Iodine and Sulphur Dioxide) is monitored with a polarized sensor to determine the water content. >> 5 0 obj It is not recommended when fat determination is to be made on same sample. /Contents [ 8 0 R 9 0 R 10 0 R 11 0 R 12 0 R 13 0 R 14 0 R 15 0 R ] How can I put the batch number on the printout from my moisture analysis? It should be thermostatically controlled and can operate at the temperature of 110oC +- 5oC (230 +- 9oF). If the presence of low molecular weight fatty acids is suspected, it may be necessary to use other tests. >> How can I avoid errors when I'm recording results and doing calculations? /Contents 23 0 R Any combination of filter and full text search is possible. \& vU_r:K~q0. 2. Dry for 3 h at 105 C. 0 USP <731> ("Loss on Drying"), AOAC and ISO describe the thermogravimetric method using a drying oven as a standard procedure for determining moisture content. AASHTO T 255/T 265 (13) /CropBox [ 0 0 617 792 ] Downloads 45 in wood or pulp, ATRO is commonly used. It is one of the widely used methods for determining the moisture content. This is either performed volumetrically, with the addition of the reagent measured, or coulometrically, where the reaction is driven in-situ and is proportional to electrical current applied. A METTLER TOLEDO instrument provides comparable and traceable results in less than 15 minutes. /T1_2 18 0 R Dry content is the amount of solids which are left after drying given as a percentage of the sample's original (wet) weight. It is defined as the mass ratio of pore water to solids and generally expressed as a percentage that shows the amount of moisture content present in that soil sample. 6 0 obj You can do this either through the ID management functionality on our moisture analyzers or in the differential weighing application on our balances. WAQTC /Parent 1 0 R The objectives of this study were: (1) to determine the effectof air oven drying methods on the moisture content of ground and whole pearl millet grain inthe moisture content range of 11.00-41.00% (w.b. The remaining dry mass is weighed to determine the loss in mass. Moisture Content represents the quality of any sample.